Blog Post

Technical Sheet: Controlling temperature and pressure during hot isostatic pressing (HIP)

Viviane Kettermann Fernandes • Apr. 20, 2022

Technical Sheet: Controlling temperature and pressure during hot isostatic pressing (HIP)


Tight tolerances are often requested when processing a component since they are very desirable for quality control, considering mechanical and dimensional tolerances, as well as time or resource savings. However, before defining the desired tolerances or ranges within which the equipment should work, it is important to understand what are the limitations of it and which physical mechanisms will happen during the process that cannot be controlled. With that in mind, this article will be about some aspects of how stable a hot isostatic pressing process can be, focused upon temperature and pressure control. 

The main process parameters of hot isostatic pressing are the temperature, pressure and the dwell time. Besides that, heating and cooling rates can play an important role in the material or part properties, depending on the rates’ order of magnitude.

Therefore, to maintain reliability and control to the system in terms of temperature and pressure, two main hardware features of the machine should be taken care, respectively: the thermocouples and the sealing surfaces.

Yet for industrial applications, tight tolerances are often not required during HIP processes [1], it depends highly on the parameters applied during the process, being more difficult to maintain it at high pressures and high temperatures.

In the next sections it will be described how the use of different thermocouples can influence the measurement of temperature and its assurance. Further, how maintenance of the sealing surfaces provides a good pressure stability, yet small instabilities in pressure are normal in HIP due to densification mechanisms, especially for encapsulated parts.


Temperature accuracy

Before talking about thermocouples, it is important to mention that HIP vessels are distributed in different thermal zones, like floors, as showed in Figure 1. Number of thermal zones will depend on the size of the machine and how it is constructed. Each zone presents more than one thermocouple for redundancy.

Further, heating in hot isostatic pressing occurs not only by radiation, but as well through circulation of hot gases inside the furnace.

Between the heating elements and the pressure vessel, there is the heat shield, which prevents heat losses and protects the external hardware from the high temperatures.

Thermocouples

Thermocouples usually used in HIP vessels are Type S and Type B for control of temperature in the zones, or the pieces being treated. Type S is normally only used when special kind of certifications are required, for example for aerospace industry. Other kinds of thermocouples, such as type K, can be found in the system to control temperature of hardware parts, such as the top cover.

Thermocouple Type K: these are nickel bases thermocouples usually with 10% of chromium (+) vs nickel with 5% of aluminum and silicon (-). Applicable for oxidizing or inert atmospheres with a temperature limit up to 1260 °C. Tolerance of reading is high in comparison with Type S and B, being almost +/- 2%, depending on the composition [2].

Thermocouple Type S: It has an operational temperature up to 1480 °C, and it is platinum (-) vs platinum-10%rhodium (+). It is very stable, but must be protected from metallic and non-metallic vapor, and it is suitable for air or inert atmospheres. Tolerance of this kind of thermocouple is very small compared to the other types, in the range of +/- 0.25% [2].

Thermocouple Type B: Made of platinum with addition of rhodium (30% (+) vs. 6% (-)) suitable for use until 1700 °C. Besides the working temperature, has the advantage over the thermocouple of Type S to be more resistance to grain growth, which could result into failure. However, requires the double of tolerance rate than type S (+/- 0.5%) [2].


Heat transfer inside the vessel

When the vessel is heating, it is very possible that the upper zone will be heated up faster than the others, since the density of heated gas decreases and it dislocates up within the furnace. 

The effect of convection inside of the furnace will also depend on the pressure of the system, because with less gas the effect will be less pronounced. [3]


Pressure accuracy

To maintain the pressure of the system it is obviously important that it is leak checked. One way to avoid leakage is to perform inspection of the vessel at regular intervals to check for cracks, to prevent fatigue failure. Small cracks can already be identified in these inspections.

On a daily basis it is recommended that the furnace is maintained clean and without moisture. Both can not only damage the heating system, but also the pumping one. 

By the processing of an encapsulated powder, a slight change of pressure can be seen during the dwell stage, due to the densification process of the capsule.

With the densification and subsequent reduction of volume of the piece inside of the HIP, it is possible to observe a slightly decrease in the system pressure, depending on the load volume and on how the parts have been filled and evacuated previous to the thermomechanical process, as represented in Image 2.


Overview

HIP is very reliable and has many advantages when applied for densification as a manufacturing or post-process. However, it is important to observe that even for calibrated thermocouples, there is a margin of measurement error from 0.25 to 0.5% of the temperature. Besides that, even with new vessels that have a very good control of temperature, it is possible, especially in heating up and cooling down, to see a difference between temperatures between the top and bottom zones, due to the convection mechanism. 

Regarding pressure accuracy, small drops in pressure during dwell stage can help due to the densification of parts. This effect is more pronounced in PM cannisters, due to the low density previous HIP. 


References

[1] ATKINSON, H. V.; RICKINSON, B. Hot Isostatic Pressing.(Book). Adam Hilger, 190, 1991, S. 1991.

[2] PARK, Richard M. Thermocouple fundamentals. Course Tech., Temp, 2010, S. 2-1.

[3] MEHRA, Raman K.; MAHMOOD, Shah; RUNKEL, Joe. Temperature control of hot isostatic pressing (HIP) furnace using model predictive and risk sensitive optimal controllers. In: Proceedings of International Conference on Control Applications . IEEE, 1995. S. 949-954.

Teilen

von Daniel Guizard 10 Aug., 2022
In this special, we introduce our newest offering – Powder Metallurgy. Using our methods, we are able to produce semi-finished products by combining several interesting technologies including can manufacture, encapsulation, welding, vacuum, hot isostatic pressing (HIP) as well as CNC machining. This allows us to produce parts and material combinations that would not be possible using conventional manufacturing methods. But why do we do this? Having conversed with a multitude of customers from a variety of markets, we established that the ability to produce semi-finished products using a combination of these technologies, isn’t widely known. When presenting the idea of encapsulation via powder metallurgy, our clients already have suitable ideas and products in mind, but very few options to obtain all of the necessary technologies from one supplier. OWLHIP-PM can improve the quality of your products, reduce cost per piece (depending on the lot size to be produced), and decrease delivery times, whilst producing parts and material combinations which traditionally would have been deemed impossible. The OWLHIP-PM production chain, showing the steps which occur after powder selection and can manufacture, is as follows: First step: Powder Sourcing – Many different powders exist on the market and many of them can be used to produce OWLHIP-PM products. There are numerous combinations of suitable powders available, as well as conventional stainless, tooling, cold-working, high speed and wear-resistant steels and Fe-based alloys; further Ni, Al, Ti, and Co-based alloys. Mixing different types of powder is possible and is indeed often used to adjust and optimise the characteristics of the semi-finished product. We assist in the selection of the right powder for your product. Due to our strong network and relationship with powder manufacturers, we are also able to support you from initial prototypes through to serial production. Second step: Can Manufacture (Design/Bending/Bordering/Welding the Can) – This is naturally one of the most important steps in the process. The design of the can needs to be calculated correctly to allow for the expected shrinkage during the HIP process. Our knowledge includes the design of the can dimensions before and after HIP to use as little raw materials as possible. The can could be a simple tube, a square or even a very complex 3D structure. There are almost no limits. The welding needs to be 100% gas-tight, in order to avoid inclusions which will result in scrap parts. For this reason, every can produced with our OWLHIP-PM process is tested with a gas leakage system in order to avoid defective parts even entering the HIP process. Every can produced and supplied by OWL comes with a certificate, showing that the welding was checked according to our internal process standards. Third step: Filling – This requires knowledge about the powder, its tap density, as well as its floating behaviour. The optimum vibration frequency is used to densify the powder and provides the best possible conditions for obtaining a homogeneous semi-finished part after HIP. Fourth step: Vacuum degassing and Closing – The can is filled with powder prior to evacuation. This step will define if the powder is sintered perfectly together during the HIP process. Based on our internal process standards and the material(s) being evacuated, we apply an optimal evacuation time, according to the needs of the material. After the final vacuum level is reached, the can is closed. Fifth step: HIP Process (Hot Isostatic Pressing) - When components are treated with the Hot Isostatic Pressing (HIP) process - simultaneous application of elevated heat and pressure within an inert gas atmosphere - internal cavities and micro-porosities are eliminated through a combination of plastic deformation, flow, and diffusion bonding of the material. This section of the process is where the powder in the can transforms into a solid material. Our equipment and standards of processing are in line with leading aerospace standards, where we also hold AS/EN9100 and ISO9001 accreditations. Sixth Step: CNC Machining – The product is now suitable for almost any type of machining method suited to its final design. Quality control - Our OWLHIP-PM internal standards ensure the best quality possible. Every production step is controlled by the highest standards. Advantages of using OWLHIP-PM: Isotropic material properties Production of complex, Near-Net-Shape (NNS) parts Less subsequent CNC machining due to NNS Significantly reduced lead-times Capacity availability and continual capacity investments Optimal and significantly reduced use of raw materials International supplier network for the full array of powder needs Possibility to produce parts made from materials that are only available in powder form Production of multi-material parts is possible; to include suitable bimetallic combinations To optimise your current product portfolio, reduce usage of raw materials, or even produce parts and applications which were not possible before, please contact Daniel Guizard (dgu@owl-am.com) or David Loughlin (dlo@owl-am.com)
von Daniel Guizard 01 Juni, 2022
We did it again! Last week, 24th of May, we successfully passed the surveillance audit of our Aerospace Quality Management System EN9100 (equivalent to AS9100) also maintaining our ISO9001 status. Thanks to TÜV SÜD for this very professional audit. Excellence in Quality, through stable processes and customer orientation, have been the basis for our successes to date. It was a pleasure to have this verified externally over the course of the audit.
von Daniel Guizard 24 Mai, 2022
We offer weekly shared direct transport: UK to Germany to UK In support of our growing UK customer base, OWL AM are now offering a weekly direct shared transport service to and from our plant in Aachen, Germany. We have committed to sending a vehicle from the UK to Aachen on a fixed day each week, for the shared use of our customers. With the added foresight of the pending processing requirements, we are able to even more quickly and efficiently process your order within either the pre-booked cycle slot, or within one of our new ‘OWLHIP’ shared cycles. The parts are then quickly sent back to your site on the next available shared use direct vehicle. To book your space on the next available transport or to find out more, contact David Loughlin (dlo@owl-am.com)
von Daniel Guizard 16 Mai, 2022
OWL AM Additive Manufacturing, in the next phase of its development for Hot Isostatic Pressing (HIP) services, would like to introduce the ‘OWLHIP’ range. These processes are dedicated to support the needs of customers who require shared HIP cycles. The market has for many years been asking for a simpler, more cost-effective way of obtaining shared HIP cycles. Sending parts for a shared HIP cycle, only for them to be processed several weeks later against no guaranteed schedule, is impossible to work with. The ‘OWLHIP’ range of processes delivers against all of these needs and more. Benefits of the ‘OWLHIP’ range include: The most cost effective HIP solution for ‘small’ batch sizes – where the cost of a dedicated cycle can be prohibitive Easier to specify your processing needs – simply refer to the programme name below, no complex parameters Guaranteed lead-times Highest standards of customer service EN9100 certified Quality Management System. The OWLHIP range of processes, dedicated to shared HIP cycles: ‘OWLHIP13’ - process for the HIP densification needs of most Aluminium alloys ‘OWLHIP22’ – process for the HIP densification needs of most Titanium alloys ‘OWLHIP26’ - process for the HIP densification needs of most Steel alloys ‘OWLHIP27’ - process for the HIP densification needs of typical Cobalt alloys ‘OWLHIP28’ - process for the HIP densification needs of most Nickel alloys. To find out more, or to book your parts into our next shared HIP cycle, please either use the contact form on our website or write to us by email contact@owl-am.com
von Daniel Guizard 02 März, 2022
Happy to introduce our new Team member. Viviane Kettermann Fernandes is a Materials Engineer with experience of laser material processing, hot isostatic pressing, and heat treatment. Currently she is finishing her doctoral thesis in the field of additive manufacturing combined with thermomechanical treatments. Her expertise is in the field of material properties analysis and research and development. Viviane’s materials science knowledge will be used to good effect, supporting our customers in developing bespoke HIP programs, as well as with their needs within the fields of Powder Metallurgy and Additive Manufacturing. Welcome on-board, Viviane!
Share by: